英语翻译XRD spectra were recorded on a Rigaku Ultima-IV X-ray di
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英语翻译
XRD spectra were recorded on a Rigaku Ultima-IV X-ray diffractometer
with Ni-filtered Cu K\3radiation (\3 = 0.15418 nm) operated
at 40 kV and 40mA in air,with an environmental humidity of
around 60%.Samples were tested under diffraction angle,2\4,in
the range of 5–30◦ with a step interval of 0.5◦ min−1.The profiles
were smoothed and the background was subtracted from all of the
data.Transmission electron microscopy (TEM) analyses were performed
for the membranes stained with silver ions.SPI samples
were immersed in 0.5M AgNO3 aqueous solution overnight,then
rinsed with water and dried at room temperature for 24 h.Images
were taken on a Tecnai G2 F20 transmission electron microscope
using an accelerating voltage of 200 kV.
XRD spectra were recorded on a Rigaku Ultima-IV X-ray diffractometer
with Ni-filtered Cu K\3radiation (\3 = 0.15418 nm) operated
at 40 kV and 40mA in air,with an environmental humidity of
around 60%.Samples were tested under diffraction angle,2\4,in
the range of 5–30◦ with a step interval of 0.5◦ min−1.The profiles
were smoothed and the background was subtracted from all of the
data.Transmission electron microscopy (TEM) analyses were performed
for the membranes stained with silver ions.SPI samples
were immersed in 0.5M AgNO3 aqueous solution overnight,then
rinsed with water and dried at room temperature for 24 h.Images
were taken on a Tecnai G2 F20 transmission electron microscope
using an accelerating voltage of 200 kV.
XRD spectra were recorded on a Rigaku Ultima-IV X-ray diffractometer with Ni-filtered Cu K\x03radiation (\x03 = 0.15418 nm) operated at 40 kV and 40mA in air, with an environmental humidity of around 60%. Samples were tested under diffraction angle, 2\x04, in the range of 5–30◦ with a step interval of 0.5◦ min−1. The profiles were smoothed and the background was subtracted from all of the data. Transmission electron microscopy(TEM) analyses were performed for the membranes stained with silver ions. SPI samples were immersed in 0.5M AgNO3 aqueous solution overnight, then
rinsed with water and dried at room temperature for 24h. Images
were taken on a Tecnai G2 F20 transmission electron microscope
using an accelerating voltage of 200 kV.
常规空气中,保持工作电压40kV、电流40mA,室内湿度(或周围湿度)60%左右,经镍滤过处理铜K\x03量级(\x03量级=0.15418nm)辐射,采用日本理学(株式会社)创世纪IV型X光衍射计记录X射线衍射(XRD)光谱.保持衍射角(量级2\x04)5-30°间、阶距0.5°/min,对样本(或:样品)进行测试.对剖面进行除障平滑处理,所有数据予背景剪影.待银离子着色后,用透射电子显微镜(TEM)对染色膜片分析处理.将磺化聚酰亚胺(SPI)样品浸入0.5mol/L的硝酸银(AgNO3)水溶液中、浸泡一夜,次日水冲洗,常温晾晒24小时置干.然后施加200kV加速电压、经Tecnai G2 F20透射电子显微镜拍摄成像.
注:
XRD=X-Ray Diffraction, X射线衍射
SPI=Sulfonated polyimides,磺化聚酰亚胺
0.5M,M=mol/L
Tecnai,FEI公司透电显微镜产品品牌
供参
rinsed with water and dried at room temperature for 24h. Images
were taken on a Tecnai G2 F20 transmission electron microscope
using an accelerating voltage of 200 kV.
常规空气中,保持工作电压40kV、电流40mA,室内湿度(或周围湿度)60%左右,经镍滤过处理铜K\x03量级(\x03量级=0.15418nm)辐射,采用日本理学(株式会社)创世纪IV型X光衍射计记录X射线衍射(XRD)光谱.保持衍射角(量级2\x04)5-30°间、阶距0.5°/min,对样本(或:样品)进行测试.对剖面进行除障平滑处理,所有数据予背景剪影.待银离子着色后,用透射电子显微镜(TEM)对染色膜片分析处理.将磺化聚酰亚胺(SPI)样品浸入0.5mol/L的硝酸银(AgNO3)水溶液中、浸泡一夜,次日水冲洗,常温晾晒24小时置干.然后施加200kV加速电压、经Tecnai G2 F20透射电子显微镜拍摄成像.
注:
XRD=X-Ray Diffraction, X射线衍射
SPI=Sulfonated polyimides,磺化聚酰亚胺
0.5M,M=mol/L
Tecnai,FEI公司透电显微镜产品品牌
供参
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